PDB entry 1la6

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HEADER    OXYGEN STORAGE/TRANSPORT                28-MAR-02   1LA6              
TITLE     THE CRYSTAL STRUCTURE OF TREMATOMUS NEWNESI HEMOGLOBIN IN A           
TITLE    2 PARTIAL HEMICHROME STATE                                             
COMPND    MOL_ID: 1;                                                            
COMPND   2 MOLECULE: HEMOGLOBIN ALPHA-1 CHAIN;                                  
COMPND   3 CHAIN: A;                                                            
COMPND   4 MOL_ID: 2;                                                           
COMPND   5 MOLECULE: HEMOGLOBIN BETA-1/2 CHAIN;                                 
COMPND   6 CHAIN: B                                                             
SOURCE    MOL_ID: 1;                                                            
SOURCE   2 ORGANISM_SCIENTIFIC: TREMATOMUS NEWNESI;                             
SOURCE   3 ORGANISM_COMMON: ANTARCTIC FISH;                                     
SOURCE   4 MOL_ID: 2;                                                           
SOURCE   5 ORGANISM_SCIENTIFIC: TREMATOMUS NEWNESI;                             
SOURCE   6 ORGANISM_COMMON: ANTARCTIC FISH                                      
KEYWDS    HEMICHROME, BISHISTIDINE COMPLEX                                      
EXPDTA    X-RAY DIFFRACTION                                                     
AUTHOR    A.RICCIO,L.VITAGLIANO,G.DI PRISCO,A.ZAGARI,L.MAZZARELLA               
REVDAT   1   31-JUL-02 1LA6    0                                                
JRNL        AUTH   A.RICCIO,L.VITAGLIANO,G.DI PRISCO,A.ZAGARI,                  
JRNL        AUTH 2 L.MAZZARELLA                                                 
JRNL        TITL   THE CRYSTAL STRUCTURE OF A TETRAMERIC HEMOGLOBIN             
JRNL        TITL 2 IN A PARTIAL HEMICHROME STATE                                
JRNL        REF    PROC.NATL.ACAD.SCI.USA        V.  99  9801 2002              
JRNL        REFN   ASTM PNASA6  US ISSN 0027-8424                               
REMARK   1                                                                      
REMARK   1 REFERENCE 1                                                          
REMARK   1  AUTH   A.RICCIO,L.VITAGLIANO,G.DI PRISCO,A.ZAGARI,                  
REMARK   1  AUTH 2 L.MAZZARELLA                                                 
REMARK   1  TITL   LIGANDED AND UNLIGANDED FORMS OF ANTARCTIC FISH              
REMARK   1  TITL 2 HAEMOGLOBINS IN POLYETHYLENE GLYCOL:                         
REMARK   1  TITL 3 CRYSTALLIZATION OF AN R-STATE HAEMICHROME                    
REMARK   1  TITL 4 INTERMEDIATE                                                 
REMARK   1  REF    ACTA CRYSTALLOGR.             V.  57  1144 2001              
REMARK   1  REFN   ASTM ACCRA9  DK ISSN 0365-110X                               
REMARK   1 REFERENCE 2                                                          
REMARK   1  AUTH   L.MAZZARELLA,R.D'AVINO,G.DI PRISCO,C.SAVINO,                 
REMARK   1  AUTH 2 L.VITAGLIANO,P.C.E.MOODY,A.ZAGARI                            
REMARK   1  TITL   CRYSTAL STRUCTURE OF TREMATOMUS NEWNESI                      
REMARK   1  TITL 2 HAEMOGLOBIN RE-OPENS THE ROOT EFFECT QUESTION                
REMARK   1  REF    J.MOL.BIOL.                   V. 287   897 1999              
REMARK   1  REFN   ASTM JMOBAK  UK ISSN 0022-2836                               
REMARK   2                                                                      
REMARK   2 RESOLUTION. 2.00 ANGSTROMS.                                          
REMARK   3                                                                      
REMARK   3 REFINEMENT.                                                          
REMARK   3   PROGRAM     : X-PLOR 3.1                                           
REMARK   3   AUTHORS     : BRUNGER                                              
REMARK   3                                                                      
REMARK   3  DATA USED IN REFINEMENT.                                            
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.00                           
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 12.00                          
REMARK   3   DATA CUTOFF            (SIGMA(F)) : 2.000                          
REMARK   3   DATA CUTOFF HIGH         (ABS(F)) : NULL                           
REMARK   3   DATA CUTOFF LOW          (ABS(F)) : NULL                           
REMARK   3   COMPLETENESS (WORKING+TEST)   (%) : NULL                           
REMARK   3   NUMBER OF REFLECTIONS             : 23191                          
REMARK   3                                                                      
REMARK   3  FIT TO DATA USED IN REFINEMENT.                                     
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT                      
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM                          
REMARK   3   R VALUE            (WORKING SET) : 0.179                           
REMARK   3   FREE R VALUE                     : 0.212                           
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : NULL                            
REMARK   3   FREE R VALUE TEST SET COUNT      : 2280                            
REMARK   3   ESTIMATED ERROR OF FREE R VALUE  : NULL                            
REMARK   3                                                                      
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.                                  
REMARK   3   TOTAL NUMBER OF BINS USED           : NULL                         
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : NULL                         
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : NULL                         
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : NULL                         
REMARK   3   REFLECTIONS IN BIN    (WORKING SET) : NULL                         
REMARK   3   BIN R VALUE           (WORKING SET) : NULL                         
REMARK   3   BIN FREE R VALUE                    : NULL                         
REMARK   3   BIN FREE R VALUE TEST SET SIZE  (%) : NULL                         
REMARK   3   BIN FREE R VALUE TEST SET COUNT     : NULL                         
REMARK   3   ESTIMATED ERROR OF BIN FREE R VALUE : NULL                         
REMARK   3                                                                      
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.                    
REMARK   3   PROTEIN ATOMS            : 2154                                    
REMARK   3   NUCLEIC ACID ATOMS       : 0                                       
REMARK   3   HETEROGEN ATOMS          : 88                                      
REMARK   3   SOLVENT ATOMS            : 71                                      
REMARK   3                                                                      
REMARK   3  B VALUES.                                                           
REMARK   3   FROM WILSON PLOT           (A**2) : NULL                           
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL                           
REMARK   3   OVERALL ANISOTROPIC B VALUE.                                       
REMARK   3    B11 (A**2) : NULL                                                 
REMARK   3    B22 (A**2) : NULL                                                 
REMARK   3    B33 (A**2) : NULL                                                 
REMARK   3    B12 (A**2) : NULL                                                 
REMARK   3    B13 (A**2) : NULL                                                 
REMARK   3    B23 (A**2) : NULL                                                 
REMARK   3                                                                      
REMARK   3  ESTIMATED COORDINATE ERROR.                                         
REMARK   3   ESD FROM LUZZATI PLOT        (A) : NULL                            
REMARK   3   ESD FROM SIGMAA              (A) : NULL                            
REMARK   3   LOW RESOLUTION CUTOFF        (A) : NULL                            
REMARK   3                                                                      
REMARK   3  CROSS-VALIDATED ESTIMATED COORDINATE ERROR.                         
REMARK   3   ESD FROM C-V LUZZATI PLOT    (A) : NULL                            
REMARK   3   ESD FROM C-V SIGMAA          (A) : NULL                            
REMARK   3                                                                      
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES.                                   
REMARK   3   BOND LENGTHS                 (A) : 0.010                           
REMARK   3   BOND ANGLES            (DEGREES) : 1.45                            
REMARK   3   DIHEDRAL ANGLES        (DEGREES) : 19.70                           
REMARK   3   IMPROPER ANGLES        (DEGREES) : 1.44                            
REMARK   3                                                                      
REMARK   3  ISOTROPIC THERMAL MODEL : ISOTROPIC                                 
REMARK   3                                                                      
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.    RMS    SIGMA                
REMARK   3   MAIN-CHAIN BOND              (A**2) : NULL  ; NULL                 
REMARK   3   MAIN-CHAIN ANGLE             (A**2) : NULL  ; NULL                 
REMARK   3   SIDE-CHAIN BOND              (A**2) : NULL  ; NULL                 
REMARK   3   SIDE-CHAIN ANGLE             (A**2) : NULL  ; NULL                 
REMARK   3                                                                      
REMARK   3  NCS MODEL : NULL                                                    
REMARK   3                                                                      
REMARK   3  NCS RESTRAINTS.                         RMS   SIGMA/WEIGHT          
REMARK   3   GROUP  1  POSITIONAL            (A) : NULL  ; NULL                 
REMARK   3   GROUP  1  B-FACTOR           (A**2) : NULL  ; NULL                 
REMARK   3                                                                      
REMARK   3  PARAMETER FILE  1  : NULL                                           
REMARK   3  TOPOLOGY FILE  1   : NULL                                           
REMARK   3                                                                      
REMARK   3  OTHER REFINEMENT REMARKS: NULL                                      
REMARK   4                                                                      
REMARK   4 1LA6 COMPLIES WITH FORMAT V. 3.0, 1-DEC-2006                         
REMARK   4                                                                      
REMARK   4 THIS IS THE REMEDIATED VERSION OF THIS PDB ENTRY.                    
REMARK   4 REMEDIATED DATA FILE REVISION 3.100 (2007-03-17)                     
REMARK 100                                                                      
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB .                              
REMARK 100 THE RCSB ID CODE IS RCSB015788.                                      
REMARK 200                                                                      
REMARK 200 EXPERIMENTAL DETAILS                                                 
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION                  
REMARK 200  DATE OF DATA COLLECTION        : 30-MAR-2000                        
REMARK 200  TEMPERATURE           (KELVIN) : 293.0                              
REMARK 200  PH                             : 7.60                               
REMARK 200  NUMBER OF CRYSTALS USED        : 1                                  
REMARK 200                                                                      
REMARK 200  SYNCHROTRON              (Y/N) : N                                  
REMARK 200  RADIATION SOURCE               : ROTATING ANODE                     
REMARK 200  BEAMLINE                       : NULL                               
REMARK 200  X-RAY GENERATOR MODEL          : ENRAF-NONIUS FR571                 
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M                                  
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.5418                             
REMARK 200  MONOCHROMATOR                  : MIRRORS                            
REMARK 200  OPTICS                         : MIRRORS                            
REMARK 200                                                                      
REMARK 200  DETECTOR TYPE                  : IMAGE PLATE                        
REMARK 200  DETECTOR MANUFACTURER          : MACSCIENCE                         
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : DENZO                              
REMARK 200  DATA SCALING SOFTWARE          : SCALEPACK                          
REMARK 200                                                                      
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 27020                              
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.000                              
REMARK 200  RESOLUTION RANGE LOW       (A) : 12.000                             
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : -3.000                             
REMARK 200                                                                      
REMARK 200 OVERALL.                                                             
REMARK 200  COMPLETENESS FOR RANGE     (%) : 92.8                               
REMARK 200  DATA REDUNDANCY                : NULL                               
REMARK 200  R MERGE                    (I) : 0.07700                            
REMARK 200  R SYM                      (I) : NULL                               
REMARK 200   FOR THE DATA SET  : NULL                               
REMARK 200                                                                      
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.                                     
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.00                     
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.15                     
REMARK 200  COMPLETENESS FOR SHELL     (%) : 87.0                               
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL                               
REMARK 200  R MERGE FOR SHELL          (I) : 0.35000                            
REMARK 200  R SYM FOR SHELL            (I) : NULL                               
REMARK 200   FOR SHELL         : NULL                               
REMARK 200                                                                      
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH                              
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT        
REMARK 200 SOFTWARE USED: X-PLOR                                                
REMARK 200 STARTING MODEL: PDB ENTRY 1T1N                                       
REMARK 200                                                                      
REMARK 200 REMARK: NULL                                                         
REMARK 280                                                                      
REMARK 280 CRYSTAL                                                              
REMARK 280 SOLVENT CONTENT, VS   (%): 63.68                                     
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 3.39                     
REMARK 280                                                                      
REMARK 280 CRYSTALLIZATION CONDITIONS: MPEG 5000, SODIUM ACETATE, PH 7.6,       
REMARK 280  FREE INTERFACE DIFFUSION, TEMPERATURE 293K                          
REMARK 290                                                                      
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY                                            
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: C 1 2 1                          
REMARK 290                                                                      
REMARK 290      SYMOP   SYMMETRY                                                
REMARK 290     NNNMMM   OPERATOR                                                
REMARK 290       1555   X,Y,Z                                                   
REMARK 290       2555   -X,Y,-Z                                                 
REMARK 290       3555   1/2+X,1/2+Y,Z                                           
REMARK 290       4555   1/2-X,1/2+Y,-Z                                          
REMARK 290                                                                      
REMARK 290     WHERE NNN -> OPERATOR NUMBER                                     
REMARK 290           MMM -> TRANSLATION VECTOR                                  
REMARK 290                                                                      
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS                            
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM             
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY                
REMARK 290 RELATED MOLECULES.                                                   
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000            
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000            
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000            
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000            
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000        0.00000            
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000            
REMARK 290   SMTRY1   3  1.000000  0.000000  0.000000       44.92650            
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000       44.09500            
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000        0.00000            
REMARK 290   SMTRY1   4 -1.000000  0.000000  0.000000       44.92650            
REMARK 290   SMTRY2   4  0.000000  1.000000  0.000000       44.09500            
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000            
REMARK 290                                                                      
REMARK 290 REMARK: NULL                                                         
REMARK 300                                                                      
REMARK 300 BIOMOLECULE: 1                                                       
REMARK 300 THIS ENTRY CONTAINS THE CRYSTALLOGRAPHIC ASYMMETRIC UNIT             
REMARK 300 WHICH CONSISTS OF 2 CHAIN(S). SEE REMARK 350 FOR                     
REMARK 300 INFORMATION ON GENERATING THE BIOLOGICAL MOLECULE(S).                
REMARK 350                                                                      
REMARK 350 GENERATING THE BIOMOLECULE                                           
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN           
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE                
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS          
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND                          
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.                               
REMARK 350                                                                      
REMARK 350 BIOMOLECULE: 1                                                       
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B                                  
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000            
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000            
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000            
REMARK 350   BIOMT1   2 -1.000000  0.000000  0.000000        0.00000            
REMARK 350   BIOMT2   2  0.000000  1.000000  0.000000        0.00000            
REMARK 350   BIOMT3   2  0.000000  0.000000 -1.000000        0.00000            
REMARK 465                                                                      
REMARK 465 MISSING RESIDUES                                                     
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE                       
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN               
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)                
REMARK 465                                                                      
REMARK 465   M RES C SSSEQI                                                     
REMARK 465     SER B    43                                                      
REMARK 465     GLY B    44                                                      
REMARK 465     PHE B    45                                                      
REMARK 465     GLY B    46                                                      
REMARK 465     ASN B    47                                                      
REMARK 465     LEU B    48                                                      
REMARK 465     TYR B    49                                                      
REMARK 465     ASN B    50                                                      
REMARK 465     ALA B    51                                                      
REMARK 465     GLU B    52                                                      
REMARK 465     GLY B    53                                                      
REMARK 465     GLN B   144                                                      
REMARK 465     TYR B   145                                                      
REMARK 465     HIS B   146                                                      
REMARK 500                                                                      
REMARK 500 GEOMETRY AND STEREOCHEMISTRY                                         
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT                     
REMARK 500                                                                      
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.                            
REMARK 500                                                                      
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI                             
REMARK 500   CZ   ARG A    11     O    HOH     201              1.21            
REMARK 500   NH1  ARG A    11     O    HOH     201              1.23            
REMARK 500   NH2  ARG A    11     O    HOH     201              1.37            
REMARK 500  FE    HEM A   143     C    CMO     144              1.86            
REMARK 500                                                                      
REMARK 500 GEOMETRY AND STEREOCHEMISTRY                                         
REMARK 500 SUBTOPIC: COVALENT BOND LENGTHS                                      
REMARK 500                                                                      
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES              
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE               
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN               
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).                 
REMARK 500                                                                      
REMARK 500 STANDARD TABLE:                                                      
REMARK 500 FORMAT: (10X,I3,1X,2(A3,1X,A1,I4,A1,1X,A4,3X),F6.3)                  
REMARK 500                                                                      
REMARK 500 EXPECTED VALUES: ENGH AND HUBER, 1991                                
REMARK 500                                                                      
REMARK 500  M RES CSSEQI ATM1   RES CSSEQI ATM2   DEVIATION                     
REMARK 500    MET A  82   SD    MET A  82   CE     0.059                        
REMARK 500    MET B  18   SD    MET B  18   CE    -0.062                        
REMARK 500    MET B  78   SD    MET B  78   CE    -0.053                        
REMARK 500                                                                      
REMARK 500 GEOMETRY AND STEREOCHEMISTRY                                         
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES                                       
REMARK 500                                                                      
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES              
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE               
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN               
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).                 
REMARK 500                                                                      
REMARK 500 STANDARD TABLE:                                                      
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)              
REMARK 500                                                                      
REMARK 500 EXPECTED VALUES: ENGH AND HUBER, 1991                                
REMARK 500                                                                      
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3                                     
REMARK 500    TYR A  90   N   -  CA  -  C   ANGL. DEV. =  7.7 DEGREES           
REMARK 500    MET A 113   N   -  CA  -  C   ANGL. DEV. =  7.6 DEGREES           
REMARK 900                                                                      
REMARK 900 RELATED ENTRIES                                                      
REMARK 900 RELATED ID: 1T1N   RELATED DB: PDB                                   
REMARK 900 PDB-ID 1T1N CONTAINS THE SAME PROTEIN FULLY COMPLEXED WITH           
REMARK 900 CO                                                                   
DBREF  1LA6 A    1   142  UNP    P45718   HBA1_TRENE       1    142             
DBREF  1LA6 B    1   146  UNP    P45720   HBB_TRENE        1    146             
SEQRES   1 A  142  SER LEU SER ASP LYS ASP LYS ALA ALA VAL ARG ALA LEU          
SEQRES   2 A  142  TRP SER LYS ILE GLY LYS SER SER ASP ALA ILE GLY ASN          
SEQRES   3 A  142  ASP ALA LEU SER ARG MET ILE VAL VAL TYR PRO GLN THR          
SEQRES   4 A  142  LYS ILE TYR PHE SER HIS TRP PRO ASP VAL THR PRO GLY          
SEQRES   5 A  142  SER PRO ASN ILE LYS ALA HIS GLY LYS LYS VAL MET GLY          
SEQRES   6 A  142  GLY ILE ALA LEU ALA VAL SER LYS ILE ASP ASP LEU LYS          
SEQRES   7 A  142  THR GLY LEU MET GLU LEU SER GLU GLN HIS ALA TYR LYS          
SEQRES   8 A  142  LEU ARG VAL ASP PRO SER ASN PHE LYS ILE LEU ASN HIS          
SEQRES   9 A  142  CYS ILE LEU VAL VAL ILE SER THR MET PHE PRO LYS GLU          
SEQRES  10 A  142  PHE THR PRO GLU ALA HIS VAL SER LEU ASP LYS PHE LEU          
SEQRES  11 A  142  SER GLY VAL ALA LEU ALA LEU ALA GLU ARG TYR ARG              
SEQRES   1 B  146  VAL GLU TRP THR ASP LYS GLU ARG SER ILE ILE SER ASP          
SEQRES   2 B  146  ILE PHE SER HIS MET ASP TYR ASP ASP ILE GLY PRO LYS          
SEQRES   3 B  146  ALA LEU SER ARG CYS LEU VAL VAL TYR PRO TRP THR GLN          
SEQRES   4 B  146  ARG TYR PHE SER GLY PHE GLY ASN LEU TYR ASN ALA GLU          
SEQRES   5 B  146  GLY ILE MET SER ASN ALA ASN VAL ALA ALA HIS GLY ILE          
SEQRES   6 B  146  LYS VAL LEU HIS GLY LEU ASP ARG GLY MET LYS ASN MET          
SEQRES   7 B  146  ASP ASN ILE ALA ASP ALA TYR THR ASP LEU SER THR LEU          
SEQRES   8 B  146  HIS SER GLU LYS LEU HIS VAL ASP PRO ASP ASN PHE LYS          
SEQRES   9 B  146  LEU LEU SER ASP CYS ILE THR ILE VAL LEU ALA ALA LYS          
SEQRES  10 B  146  MET GLY HIS ALA PHE THR ALA GLU THR GLN GLY ALA PHE          
SEQRES  11 B  146  GLN LYS PHE LEU ALA ALA VAL VAL SER ALA LEU GLY LYS          
SEQRES  12 B  146  GLN TYR HIS                                                  
HET    ACE  A   0       3                                                       
HET    HEM  A 143      43                                                       
HET    CMO    144       2                                                       
HET    HEM  B 147      43                                                       
HETNAM     ACE ACETYL GROUP                                                     
HETNAM     HEM PROTOPORPHYRIN IX CONTAINING FE                                  
HETNAM     CMO CARBON MONOXIDE                                                  
HETSYN     HEM HEME                                                             
FORMUL   3  ACE    C2 H4 O                                                      
FORMUL   4  HEM    2(C34 H32 FE N4 O4)                                          
FORMUL   5  CMO    C O                                                          
FORMUL   7  HOH   *69(H2 O)                                                     
HELIX    1   1 SER A    3  GLY A   18  1                                  16    
HELIX    2   2 SER A   20  TYR A   36  1                                  17    
HELIX    3   3 PRO A   37  SER A   44  5                                   8    
HELIX    4   4 SER A   53  LYS A   73  1                                  21    
HELIX    5   5 ASP A   76  LEU A   81  1                                   6    
HELIX    6   6 LEU A   81  TYR A   90  1                                  10    
HELIX    7   7 ASP A   95  SER A   97  5                                   3    
HELIX    8   8 ASN A   98  PHE A  114  1                                  17    
HELIX    9   9 THR A  119  GLU A  139  1                                  21    
HELIX   10  10 ARG A  140  ARG A  142  5                                   3    
HELIX   11  11 THR B    4  HIS B   17  1                                  14    
HELIX   12  12 ASP B   19  TYR B   35  1                                  17    
HELIX   13  13 PRO B   36  PHE B   42  5                                   7    
HELIX   14  14 ASN B   57  ASN B   77  1                                  21    
HELIX   15  15 ASN B   80  TYR B   85  1                                   6    
HELIX   16  16 TYR B   85  LYS B   95  1                                  11    
HELIX   17  17 PRO B  100  GLY B  119  1                                  20    
HELIX   18  18 HIS B  120  PHE B  122  5                                   3    
HELIX   19  19 THR B  123  LYS B  143  1                                  21    
LINK        FE   HEM B 147                 NE2 HIS B  92                        
LINK        FE   HEM B 147                 NE2 HIS B  63                        
LINK        FE   HEM A 143                 NE2 HIS A  88                        
LINK         C   ACE A   0                 N   SER A   1                        
CRYST1   89.853   88.190   55.142  90.00  97.79  90.00 C 1 2 1       4          
ORIGX1      1.000000  0.000000  0.000000        0.00000                         
ORIGX2      0.000000  1.000000  0.000000        0.00000                         
ORIGX3      0.000000  0.000000  1.000000        0.00000                         
SCALE1      0.011130  0.000000  0.001520        0.00000                         
SCALE2      0.000000  0.011340  0.000000        0.00000                         
SCALE3      0.000000  0.000000  0.018300        0.00000